CHEM462/562ഀ

Spectrometer instructionsഀ

Part 1: Determination of the proton 90 degree pulse:ഀ

Excel spreadsheet for Pulsewidth increment: 2 microsecondsഀ

Excel spreadsheet for Pulsewidth increment: 5 microsecondsഀ

ഀ Formula used in Excel: I = I₀ * [sin (PW * pi / PW₁₈₀) * exp (- PW / P_decay)]ഀ

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with:		PW	= pulse width (in microseconds) ഀ
		pi / PW180	= conversion factor: microseconds -> radiansഀ
		Pdecay	= decay of pulse power for long pulses ഀ

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Part 2: T₁ relaxation: Use I = A - I₀ * exp (- D2 / T₁)ഀ

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Part 3: T₂ relaxation: Use I = I₀ * exp (D2 / T₂)           ഀ

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Part 4: Nuclear Overhauser Enhancement:            ഀ
           NOE / NOESY data for Cellobiose Octaacetateഀ ഀ